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山东省微山县郗山稀土矿床成矿年代学新进展

张鹏 刘珊珊 兰君 李衣鑫 邢楠 刘敬杰 刘袁坤 康志强 杨锋

张鹏, 刘珊珊, 兰君, 李衣鑫, 邢楠, 刘敬杰, 刘袁坤, 康志强, 杨锋. 山东省微山县郗山稀土矿床成矿年代学新进展[J]. 地质科技通报, 2024, 43(1): 51-62. doi: 10.19509/j.cnki.dzkq.2022.0265
引用本文: 张鹏, 刘珊珊, 兰君, 李衣鑫, 邢楠, 刘敬杰, 刘袁坤, 康志强, 杨锋. 山东省微山县郗山稀土矿床成矿年代学新进展[J]. 地质科技通报, 2024, 43(1): 51-62. doi: 10.19509/j.cnki.dzkq.2022.0265
ZHANG Peng, LIU Shanshan, LAN Jun, LI Yixin, XING Nan, LIU Jingjie, LIU Yuankun, KANG Zhiqiang, YANG Feng. New progress in the metallogenic chronology of the Chishan REE deposit in Weishan County, Shandong Province[J]. Bulletin of Geological Science and Technology, 2024, 43(1): 51-62. doi: 10.19509/j.cnki.dzkq.2022.0265
Citation: ZHANG Peng, LIU Shanshan, LAN Jun, LI Yixin, XING Nan, LIU Jingjie, LIU Yuankun, KANG Zhiqiang, YANG Feng. New progress in the metallogenic chronology of the Chishan REE deposit in Weishan County, Shandong Province[J]. Bulletin of Geological Science and Technology, 2024, 43(1): 51-62. doi: 10.19509/j.cnki.dzkq.2022.0265

山东省微山县郗山稀土矿床成矿年代学新进展

doi: 10.19509/j.cnki.dzkq.2022.0265
基金项目: 

山东省自然资源厅基金项目 鲁勘字(2018)30号

山东省地矿局科技创新项目 KC202104

山东省地矿局科技创新项目 KY202207

广西研究生教育创新计划项目 YCBZ2022119

广西研究生教育创新计划项目 YCSW2022313

详细信息
    作者简介:

    张鹏, E-mail: zhang_6999@163.com

    通讯作者:

    兰君, E-mail: lanjun56@126.com

  • 中图分类号: P618.7;P597

New progress in the metallogenic chronology of the Chishan REE deposit in Weishan County, Shandong Province

More Information
  • 摘要:

    山东省微山县郗山稀土矿床位于华北板块东南缘,是一个以轻稀土为主的岩浆热液型稀土矿床,目前为我国第三大轻稀土矿床,对其成矿年龄还存在争议。为此,以郗山稀土矿最新勘探钻孔矿石样品为研究对象,通过野外调查、矿物学和年代学研究,采用氟碳铈矿Th-Pb同位素定年精确厘定了郗山稀土矿的成矿年代。5件氟碳铈矿Th-Pb同位素定年结果表明,郗山稀土矿床成矿时代可分为2期:早期为(125.5±0.5)~(122.2±0.5)Ma,晚期为(112.3±0.6)Ma,其中早期年龄与前人得出的矿床成矿年龄基本一致,而晚期成矿年龄则是首次报道,表明郗山稀土矿床可能存在2期成矿活动,值得关注并开展进一步工作。

     

  • 图 1  鲁西区域地质简图(底图据文献[20]修改)

    Figure 1.  Geological sketch of the Luxi Block

    图 2  郗山稀土矿床地质图(含本次勘探线及钻孔位置) (底图据文献[31]修改)

    Figure 2.  Geological map of the Chishan REE deposit

    图 3  郗山稀土矿床岩心矿石样品主要矿物镜下显微照片(a~e为正交偏光,f为单偏光)

    Bsn.氟碳铈矿;Py.黄铁矿;Gn.方铅矿;Sp.闪锌矿;Cp.黄铜矿;Mo.辉钼矿;Qtz.石英;Pth.条纹长石;Kp.钾长石;Cal.方解石;Fl.萤石;Brt.重晶石

    Figure 3.  Microscopic photographs of the main minerals indrillhole ore samples from the Chishan REE deposit

    图 4  郗山矿床岩心样品典型稀土矿物扫描电镜照片(a, b)及TIMA矿物相分布图(c, d)

    Par.氟碳钙铈矿;Bsn.氟碳铈矿;Cal.方解石;Brt.重晶石;Py.黄铁矿;Fl.萤石;Ap.磷灰石;Qtz.石英;Dol(Fe).铁白云石

    Figure 4.  Scanning electron microscope photographs(a, b)and TIMA mineral distributions(c, d) of rare earth minerals in the drillhole samples from the Chishan deposit

    图 5  郗山稀土矿床氟碳铈矿CL图(a, c, e, g, i)以及加权平均年龄图(b, d, f, h, j)

    Figure 5.  CL images (a, c, e, g, i) and weighted mean Th-Pb ages (b, d, f, h, j) of bastnasite samples from the Chishan rare earth deposit

    表  1  郗山稀土矿床氟碳铈矿Th-Pb同位素定年结果

    Table  1.   Th-Pb isotope test results of cerium fluorocarbonate from the Chishan rare earth deposit

    分析点号 Pb Th U 同位素比值 同位素年龄/Ma
    wB/10-6 207Pb/206Pb 1σ 208Pb/232Th 1σ 208Pb/232Th 1σ
    ZK5-2-426 m-04 169.73 31 712 21.62 0.152 9 0.025 0 0.006 1 0.000 1 122.1 1
    ZK5-2-426 m-06 80.03 14 978 28.34 0.159 9 0.025 0 0.006 1 0.000 1 122.3 1
    ZK5-2-426 m-08 82.88 15 731 25.97 0.140 7 0.018 4 0.006 0 0.000 1 121.3 1
    ZK5-2-426 m-11 89.62 16 830 19.36 0.191 6 0.023 5 0.006 1 0.000 1 123.5 1
    ZK5-2-426 m-12 82.77 15 545 28.47 0.175 3 0.025 1 0.006 1 0.000 1 122.6 1
    ZK5-2-426 m-13 71.68 13 515 30.20 0.179 3 0.026 6 0.006 1 0.000 1 122.3 1
    ZK5-2-426 m-14 109.87 20 792 31.86 0.213 4 0.023 5 0.006 1 0.000 1 122.9 1
    ZK5-2-426 m-16 92.98 17 566 31.14 0.144 6 0.016 6 0.006 1 0.000 1 122.9 1
    ZK5-2-426 m-18 121.20 23 202 22.83 0.172 9 0.030 6 0.006 1 0.000 1 122.3 1
    ZK5-2-426 m-19 125.20 23 866 26.05 0.163 7 0.032 7 0.006 1 0.000 1 123.3 1
    ZK5-2-426 m-20 66.91 12 926 17.46 0.192 5 0.031 6 0.006 1 0.000 1 122.3 1
    ZK5-2-426 m-22 93.37 17 931 23.56 0.237 3 0.038 5 0.006 0 0.000 1 121.4 1
    ZK5-2-426 m-24 115.94 22 023 23.86 0.234 8 0.038 8 0.006 1 0.000 1 123.4 1
    ZK5-2-426 m-25 122.14 23 246 21.58 0.119 8 0.023 5 0.006 1 0.000 1 123.0 1
    ZK5-2-426 m-26 66.20 12 733 21.04 0.190 3 0.035 9 0.006 0 0.000 1 121.0 1
    ZK5-2-426 m-27 106.78 20 452 24.80 0.156 2 0.022 1 0.006 0 0.000 1 121.6 1
    ZK5-2-426 m-28 153.59 29 552 23.96 0.211 7 0.030 4 0.006 0 0.000 1 121.2 1
    ZK5-2-426 m-29 109.20 20 519 18.03 0.177 6 0.033 2 0.006 1 0.000 1 123.3 1
    ZK5-2-426 m-30 207.57 39 797 63.79 0.146 8 0.014 3 0.006 0 0.000 1 121.5 1
    ZK5-2-426 m-31 144.59 27 670 54.04 0.101 8 0.010 3 0.006 0 0.000 1 121.5 1
    ZK5-2-426 m-32 77.54 14 606 33.32 0.204 0 0.023 0 0.006 1 0.000 1 122.6 1
    ZK5-2-426 m-34 121.49 23 240 34.99 0.150 9 0.017 2 0.006 0 0.000 1 121.2 1
    ZK5-2-426 m-35 123.77 23 784 22.47 0.245 6 0.035 7 0.006 0 0.000 1 120.7 1
    ZK13-2-116 m-05 109.35 20 883 342.46 0.072 5 0.003 7 0.005 6 0.000 0 111.9 1
    ZK13-2-116 m-06 101.81 19 060 289.58 0.141 6 0.006 3 0.005 7 0.000 1 114.1 1
    ZK13-2-116 m-07 302.22 60 903 251.06 0.115 9 0.005 2 0.005 5 0.000 0 110.7 1
    ZK13-2-116 m-11 395.75 81 395 106.57 0.223 8 0.013 9 0.005 5 0.000 1 110.0 1
    ZK13-2-116 m-13 182.07 33 255 855.38 0.059 9 0.002 3 0.005 7 0.000 1 114.7 1
    ZK13-2-116 m-14 276.79 55 157 185.27 0.188 6 0.010 5 0.005 6 0.000 0 112.4 1
    ZK13-2-116 m-15 130.93 25 449 333.54 0.119 0 0.006 3 0.005 5 0.000 0 111.8 1
    ZK13-2-116 m-16 281.57 56 600 195.61 0.097 1 0.005 6 0.005 6 0.000 0 111.9 1
    ZK13-2-116 m-17 177.11 34 722 253.47 0.078 0 0.005 1 0.005 6 0.000 0 113.3 1
    ZK13-2-116 m-18 370.98 76 067 92.72 0.136 1 0.017 0 0.005 5 0.000 0 111.3 1
    ZK13-2-116 m-19 264.75 52 612 257.87 0.083 6 0.005 0 0.005 6 0.000 0 113.7 1
    ZK13-2-116 m-20 133.94 25 202 487.28 0.068 2 0.003 1 0.005 6 0.000 0 113.5 1
    ZK13-2-116 m-21 142.58 27 089 560.73 0.0603 0.002 6 0.005 5 0.000 0 111.5 1
    ZK13-2-116 m-22 269.79 54 743 205.44 0.079 6 0.005 1 0.005 5 0.000 0 110.8 1
    ZK13-2-116 m-23 235.59 46 987 150.72 0.130 5 0.012 0 0.005 6 0.000 0 113.0 1
    ZK13-2-116 m-24 191.67 37 228 403.45 0.096 0 0.004 0 0.005 6 0.000 0 112.7 1
    ZK13-2-116 m-29 299.06 59 755 260.20 0.103 7 0.006 2 0.005 6 0.000 1 112.7 1
    ZK13-2-402 m-01 37.75 7 085 6.40 0.606 9 0.090 3 0.006 1 0.000 1 122.6 1
    ZK13-2-402 m-02 22.41 4 244 8.78 0.483 2 0.072 4 0.006 0 0.000 1 120.7 1
    ZK13-2-402 m-03 21.64 4 032 9.17 0.356 9 0.058 1 0.006 1 0.000 1 122.9 1
    ZK13-2-402 m-04 30.85 5 588 12.76 0.725 4 0.094 8 0.006 2 0.000 1 125.5 1
    ZK13-2-402 m-06 26.80 5 041 11.34 0.278 0 0.038 5 0.006 1 0.000 1 122.6 1
    ZK13-2-402 m-08 24.99 4 731 5.64 0.793 4 0.124 4 0.006 0 0.000 1 121.4 1
    ZK13-2-402 m-10 23.13 4 227 9.04 0.797 6 0.105 6 0.006 2 0.000 1 124.0 1
    ZK13-2-402 m-11 31.96 5 922 9.98 0.523 0 0.086 0 0.006 2 0.000 1 124.1 1
    ZK13-2-402 m-12 21.74 3 969 7.23 0.834 6 0.110 3 0.006 2 0.000 1 125.3 1
    ZK13-2-402 m-13 37.47 6 933 10.42 0.204 2 0.035 7 0.006 2 0.000 1 125.1 1
    ZK13-2-402 m-14 24.51 4 591 9.10 0.466 5 0.073 9 0.006 1 0.000 1 123.2 2
    ZK13-2-402 m-16 23.04 4 340 13.20 0.674 4 0.098 0 0.006 0 0.000 1 121.6 2
    ZK13-2-402 m-18 40.98 7 456 4.54 0.995 5 0.093 6 0.006 2 0.000 1 124.7 2
    ZK13-2-402 m-19 23.91 4 474 9.03 0.537 4 0.103 1 0.006 1 0.000 1 122.8 1
    ZK13-2-402 m-20 26.26 4 881 8.11 0.720 8 0.105 5 0.006 1 0.000 1 122.9 1
    ZK13-2-402 m-21 28.81 5 108 11.60 0.706 2 0.052 9 0.006 3 0.000 1 126.0 1
    ZK13-2-402 m-24 29.84 5 612 9.61 0.402 0 0.052 5 0.006 1 0.000 1 122.5 1
    ZK13-2-402 m-25 75.82 13 883 14.67 0.566 1 0.065 6 0.006 2 0.000 1 125.8 1
    ZK13-2-402 m-26 40.69 7 538 4.45 0.367 0 0.061 2 0.006 2 0.000 1 124.8 1
    ZK13-2-402 m-27 29.76 5 503 8.35 0.851 5 0.131 1 0.006 1 0.000 1 122.9 1
    ZK13-2-402 m-30 37.49 6 847 8.66 0.908 8 0.054 6 0.006 1 0.000 1 122.0 1
    ZK13-2-402 m-33 43.66 8 132 6.21 0.348 6 0.054 2 0.006 2 0.000 1 124.6 1
    ZK13-2-402 m-35 47.13 8 701 9.04 0.510 6 0.070 1 0.006 2 0.000 1 125.0 1
    ZK11-1-379 m-01 105.59 19 182 7.05 0.664 0 0.055 2 0.006 2 0.000 1 124.8 1
    ZK11-1-379 m-03 113.78 20 587 9.90 0.694 1 0.070 2 0.006 2 0.000 1 125.3 1
    ZK11-1-379 m-04 59.00 10 639 14.30 0.677 3 0.082 5 0.006 3 0.000 1 126.3 1
    ZK11-1-379 m-07 87.66 15 911 9.60 0.829 5 0.087 8 0.006 2 0.000 1 125.6 2
    ZK11-1-379 m-08 222.80 41 099 54.83 0.141 2 0.010 7 0.006 2 0.000 1 124.0 2
    ZK11-1-379 m-09 173.10 31 776 12.03 0.441 9 0.057 4 0.006 2 0.000 1 125.4 2
    ZK11-1-379 m-10 129.58 23 688 4.35 0.896 8 0.090 9 0.006 2 0.000 1 125.1 2
    ZK11-1-379 m-11 60.02 10 814 16.76 0.743 8 0.093 3 0.006 3 0.000 1 127.6 2
    ZK11-1-379 m-12 76.39 13 858 11.47 0.775 0 0.063 9 0.006 2 0.000 1 125.4 1
    ZK11-1-379 m-13 86.23 16 008 6.85 0.587 3 0.114 8 0.006 2 0.000 1 124.3 1
    ZK11-1-379 m-15 47.49 8 748 19.71 0.489 7 0.051 7 0.006 3 0.000 1 126.2 2
    ZK11-1-379 m-16 186.35 34 545 9.17 0.582 6 0.069 9 0.006 3 0.000 1 125.9 1
    ZK11-1-379 m-18 174.30 32 015 53.08 0.191 1 0.015 0 0.006 3 0.000 1 127.3 1
    ZK11-1-379 m-19 332.72 63 297 64.01 0.169 1 0.018 4 0.006 2 0.000 1 125.1 2
    ZK11-1-379 m-20 346.23 64 157 63.69 0.155 1 0.012 4 0.006 3 0.000 1 127.6 1
    ZK11-1-379 m-22 417.94 77 323 105.74 0.216 6 0.011 0 0.006 3 0.000 1 127.2 1
    ZK11-1-379 m-24 106.66 19 794 25.08 0.385 3 0.045 0 0.006 2 0.000 1 125.2 1
    ZK11-1-379 m-25 86.77 16 181 3.26 0.867 0 0.121 9 0.006 2 0.000 1 124.7 1
    ZK11-1-379 m-26 87.90 16 204 8.48 0.426 4 0.067 4 0.006 2 0.000 1 125.5 1
    ZK11-1-379 m-27 423.09 78 096 88.39 0.183 7 0.012 0 0.006 2 0.000 1 125.5 1
    ZK11-1-379 m-28 163.98 30 423 6.06 0.855 8 0.093 2 0.006 2 0.000 1 125.2 1
    ZK11-1-379 m-29 111.39 20 459 9.51 0.564 6 0.070 0 0.006 2 0.000 1 125.6 1
    ZK11-1-379 m-31 163.49 29 910 24.16 0.321 7 0.033 2 0.006 3 0.000 1 126.7 2
    ZK11-1-379 m-32 292.56 54 666 21.20 0.534 3 0.033 1 0.006 1 0.000 1 123.8 1
    ZK11-1-379 m-33 90.64 16 301 21.14 0.700 7 0.046 2 0.006 3 0.000 1 126.7 2
    ZK11-1-379 m-34 119.21 21 803 18.15 0.746 1 0.042 6 0.006 2 0.000 1 124.9 1
    ZK11-1-379 m-36 86.29 16 001 5.71 0.864 2 0.094 1 0.006 1 0.000 1 123.6 1
    ZK11-1-628 m-06 154.70 28 199 25.34 0.619 7 0.036 0 0.006 2 0.000 1 124.3 1
    ZK11-1-628 m-07 121.40 22 632 86.35 0.214 9 0.013 1 0.006 1 0.000 1 122.1 1
    ZK11-1-628 m-08 164.29 30 261 57.80 0.123 9 0.011 1 0.006 2 0.000 1 124.3 1
    ZK11-1-628 m-12 121.90 22 711 18.43 0.509 6 0.044 1 0.006 1 0.000 1 122.6 1
    ZK11-1-628 m-17 101.47 18 694 16.02 0.241 9 0.026 6 0.006 3 0.000 1 125.9 1
    ZK11-1-628 m-19 129.40 24 081 25.87 0.371 1 0.042 1 0.006 3 0.000 1 125.8 1
    ZK11-1-628 m-20 72.46 13 594 11.42 0.396 0 0.047 0 0.006 3 0.000 1 126.6 1
    ZK11-1-628 m-25 85.39 16 227 36.94 0.701 2 0.055 7 0.006 1 0.000 1 122.1 1
    ZK11-1-628 m-29 107.05 21 539 18.44 0.818 8 0.082 9 0.006 0 0.000 1 120.4 1
    ZK11-1-628 m-32 93.06 17 772 68.23 0.281 3 0.021 7 0.006 1 0.000 1 122.9 1
    ZK11-1-628 m-34 78.60 14 962 16.45 0.598 4 0.063 0 0.006 2 0.000 1 125.1 1
    ZK11-1-628 m-35 110.10 21 089 89.53 0.116 7 0.012 2 0.006 1 0.000 1 123.1 1
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  • 收稿日期:  2022-08-15
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