Genetic mechanism of low resistance in shale analyzed by triaxial compression test
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摘要: 【目的】川南地区五峰-龙马溪组页岩气储层在多个地区出现低电阻异常现象。统计显示,低阻页岩(<10 Ω·m)与构造断裂带在空间分布上存在叠合关系。为揭示页岩电阻率与构造断裂带之间的关联机制,【方法】本文基于薄片鉴定、X-射线衍射分析、激光拉曼光谱分析、全岩沥青反射率测定以及常规物性分析等手段,确定了页岩试样的岩石学特征和地球化学特征;再基于三轴压缩物理模拟试验确定了变形过程中页岩试样电阻率的变化特征,明确了裂缝发育及盐水的侵入对页岩低阻现象的影响。【结果】结果表明:黏土矿物、黄铁矿和高热演化程度有机质相对均一的页岩试样,在饱和不同浓度盐水后,电阻率显著降低,且电阻率降低幅度(95.07% ~ 98.70%)与盐水浓度之间存在正相关关系;饱和盐水的页岩试样受压破裂后电阻率进一步降低,降低幅度介于5.7 Ω·m ~ 25.7 Ω·m(平均值为13.3 Ω·m),且页岩试样饱和盐水后的电阻率与其破裂后的电阻率符合正相关线性关系。【结论】页岩内部裂缝系统的发育后导电流体的侵入,是页岩电阻率降低的主要控制因素。页岩受压破裂后电阻率的降低幅度受到入侵溶液浓度和裂缝发育程度的双重影响。研究成果解释并补充了构造断裂带对页岩电阻率的影响机制,丰富了低阻页岩成因机制理论,对低阻页岩层段的勘探开发具有重要意义。Abstract: 【Objective】The gas shale of Wufeng-Longmaxi Formation in the southern Sichuan Basin shows the low-resistance anomaly in multiple areas. Statistical analysis reveals that the low-resistivity zone (<10 Ω·m) in the Wufeng-Longmaxi shale is spatially associated with tectonic faults. To reveal the coupling mechanism between shale resistivity and tectonic fault, 【Methods】this paper determined the petrological and geochemical characteristics of the outcrop samples obtained from the Wufenglongmaxi shale of Southern Sichuan Basin through analyses of thin-section identification, X-ray diffraction, laser Raman spectroscopy, whole-rock asphalt reflectance, and conventional physical property. Subsequently, the characteristics of shale resistivity change during the deformation were revealed using the triaxial compression tests. The impact of the fracture system generation and the conductive fluid intrusion on low-resistance shale was also clarified.【Results】The results show that the resistivity of shale samples, primarily composed of uniform clay minerals, pyrite, and organic matter with high thermal maturity, significantly decreased after being saturated with various salinity brines. There is a positive correlation between the reduction of resistivity (95.07%-98.70%) and the brine salinity. After reaching the limit of compressive strength, the resistivity of brine-saturated samples generally experienced a further resistivity decrease of 5.7 Ω·m to 25.7 Ω·m (with an average value of 13.3 Ω·m). This decrease maintained a linearly positive correlation with the resistivity observed after cracking.【Conclusion】The intrusion of conductive fluid and the generation of the fracture system in shale were the primary controlling factors for shale resistivity reduction, and the resistivity after cracking was governed by both the intruded brine salinity and the fracture density. This research elucidates and supplements the influence mechanism of tectonic fault zones on shale resistivity, enriching the theoretical framework for understanding the genesis of low-resistivity shale, and holds significant implications for exploration and development of low-resistivity shale formations.
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Key words:
- low-resistivity shale /
- low-resistivity origin /
- cracks /
- formation water
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